
1. Click the Windows Start button, then Programs, then Cary WinUV, and then
Align.
2. Click the Cary tab.
3. Set the following parameters:
Double
beam:
Normal
Y mode: %R
Ave time: 0.1
SBW: 2
Slit
height:
reduced
4. Select the Zero order check box and click OK.
Caution
The DRA should not be plugged in and operated with the instrument set to 0 nm. If it
is, the detectors will be flooded with white light, which will decrease the sensitivity of
the accessory and increase noise. If this should happen, place the DRA in a dark place
for 24 hours to allow it to recover.
5. Remove the front cap from the accessory and observe the diffuser at the
reference port. The image should be centered on the diffuser.
If it is not:
• Check that that DRA is correctly locked down onto the
instrument sample compartment floor.
• If the DRA is correctly installed, and misalignment persists,
contact your local Varian service representative.
6. Replace the sphere cap with the 'S' mark upwards.
7. Tape a card over the diffuser on the reference port to exclude light. Make sure
you do not contaminate the surface of the diffuser.
8. Check the adjustment of the Beam on to mirror M2. If necessary adjust the
horizontal alignment of the beam by loosening the screws on either side of
mirror M1 and rotating it slightly.
9. Fasten the screws.
Commenti su questo manuale