
that the instrument to be turned on and off at various times. It is important to take care
that you follow these steps as failure to do so can cause damage to your DRA.
Reflectance measurements (%R)
The sample should be homogeneous, substantially flat, and large enough to
completely cover the image. Finely powdered samples may be studied using a
powder cell
. There is also a mounting option available for small samples.
When measuring diffuse only reflectance, position the sphere cap with the 'D' mark
up. Position the 'S' mark up to measure the specular+diffuse (total) reflectance.
When performing measurements on glossy materials (high specular component), use
the protruding reference plate. The reference surface protrudes into the sphere and
behaves more nearly like a perfect diffuser. As discussed in the Differences between
the standard and sample section, you should use reference materials with similar
reflectivity and properties to the sample.
Figure 15: Reference disks supplied with the DRA. The large reference plate (a), and
the protruding reference plate (b).
Note
Parameters activated by a radio button that are not specifically mentioned in the
following procedure should be set to 'Off' (e.g., the Signal-to-noise mode radio
button). These parameters will not affect the procedure.
1. After you have carried out the Alignment procedures, turn off the instrument.
2. Plug the DRA into the instrument using the communications plug, it fits into
the green plug at the back of the instrument's sample compartment.
3. Cover the reflectance port with a PTFE reference disc.
Caution
Before turning on your instrument you must cover the reflectance port with a PTFE
reference disc to prevent damage to your DRA.
4. Install the extended sample compartment
.
5. Close the sample compartment lid.
6. Turn on the instrument, allow the instrument to initialize.
7. Click the Windows Start button, then Programs, Cary WinUV and then Scan.
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