Mantis 5000 Specifiche Pagina 38

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X mode: Stop 300
Y mode: Mode % R
Y mode: Y min -5.00
Y mode: Y max 110.00
Scan controls: Ave time (s) 0.100
Scan controls: Data interval (nm) 1.000
Scan controls: Scan rate (nm/min)600.00
Options tab
SBW/Energy: Fixed SBW ON
SBW/Energy: SBW (nm) 2.00
SBW/Energy: Beam mode Double
SBW/Energy: Slit height Reduced
Source: Lamps UV-Vis
Source: Source changeover (nm) 350.0
Baseline tab
Correction Zero baseline/correction
Autostore tab
File Storage: Storage Storage on (prompt at start)
2. Position the sphere cap with the 'S' mark up.
3. Click the Baseline button in the Scan dialog box. Follow the on-screen
prompts to perform a 100%T baseline scan and a 0%T baseline scan.
Hot Tip
When performing specular zero (%T) collect, remove the reference PTFE disc
and allow the light to be trapped by the external sample compartment.
4. Once the baseline correction is complete, the Ordinate status display in the top
left corner of the dialog box will show 'Zero baseline' in red text.
5. Clamp the sample over the reflectance port. The sample should be
homogeneous, substantially flat, and large enough to completely cover the
image.
6. Click the Start button to perform the scan of the total (specular and diffuse)
reflectance of the sample.
7. Turn the sphere cap so the 'D' mark is up, and click the Start button to collect
the diffuse-only data.
8. From the main Scan window, click the Calculator icon
to open the open
the Maths dialog box.
9. On the graph displayed, highlight the first scan (of the total reflectance) by
clicking on it. When the scan is selected, it will be highlighted in red.
10. From the Maths dialog box choose Selected Trace and then the '-' (minus)
sign.
11. On the graph displayed, highlight the second scan (of the diffuse-only
reflectance), by clicking on it. When the scan is selected, it will be highlighted
in red.
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