Mantis 5000 Specifiche Pagina 19

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Figure 14: DRA socket
10. Place the PTFE reference disc over the reflectance port.
11. Install the Extended Sample Compartment according to its instruction manual.
12. Close the sample compartment, turn on the instrument and wait for correct
initialization to be completed.
Note
Improper alignment of the DRA may prevent the Cary from finding the 656.1
nm wavelength calibration line.
Error checks
Note
Parameters activated by a radio button that are not specifically mentioned in the
following procedure should be set to 'Off' (e.g., the Signal-to-noise mode radio
button). These parameters will not affect the procedure.
1. Click the Windows Start button, then Programs, then Cary WinUV, and then
Scan.
2. Click the Setup button.
3. From the Setup menu, set the following parameters to carry out the error
checking.
Cary tab
X mode: Mode
N
anometers
X mode: Start/Stop User-set range
Y mode: Mode % R
Y mode: Y min -5.00
Y mode: Y max 110.00
Scan controls:
Ave time (s)
1.000
Scan controls:
Data interval (nm)
0.500
Scan controls:
Scan rate (nm/min)
30.000
Options tab
SBW/Energy: Fixed SBW ON
SBW/Energy: SBW (nm) 2.00
SBW/Energy: Beam mode Double
SBW/Energy: Slit height Reduced
Source: Lamps UV-Vis
Source: Source
changeover (nm)
350.0
Baseline tab
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